[關鍵詞]
[摘要]
目的 培養(yǎng)布南色林的單晶,以驗證所合成的化合物為布南色林。方法 通過溫度、質量濃度、溶劑的考察,選擇合適的條件,培養(yǎng)出大小適合X射線單晶衍射檢測的布南色林單晶。結果 通過X射線單晶衍射測定,結果顯示所得數(shù)據(jù)與文獻報道一致,證明布南色林的化學結構正確。結論 采用本法可很好地獲得大小適合X射線單晶衍射檢測的布南色林單晶,并確證了其空間結構,提示合成的布南色林結構正確。
[Key word]
[Abstract]
Objective To cultivate the single crystal of Blonanserin, and to establish the structure of Blonanserin. Method To selected the best condition by inspecting the different temperature, concentration, and solution. At this condition the single crystal size of Blonanserin fit for X-ray analysis. Results The structure of Blonanserin was accurate and the data was the same with the literature report. It proved that the structure of Blonanserin was right. Conclusion The single crystal size of Blonanserin obtained is fit for X-ray analysis and the space structure is proved right. And it suggests the structure that synthesized by our corporation be exact.
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