目的 為了更好的控制產(chǎn)品質(zhì)量，建立安腎丸的質(zhì)量標(biāo)準(zhǔn)。方法 采用薄層色譜法對(duì)制劑中的肉蓯蓉、補(bǔ)骨脂、白術(shù)進(jìn)行了定性鑒別，并采用高效液相色譜法測(cè)定苦杏仁苷。結(jié)果 薄層色譜中的特征斑點(diǎn)明顯。苦杏仁苷在10.25～512.50 μg線性關(guān)系良好（r=0.999 9），平均回收率為99.78%，RSD值為1.16%（n=6）。結(jié)論 建立的方法專屬性強(qiáng)、重復(fù)性好，準(zhǔn)確簡(jiǎn)便，可有效地控制安腎丸的質(zhì)量。

Objective To establish a quality standards for the quality control of Anshen Pill. Methods The qualitative identification of Cistanches Herba, Psoraleae Fructus, and Atractylodis Macrocephalae Rhizoma in the preparation was carried out by TLC, and the content of amygdalin was determined by HPLC. Results The TLC characteristic spots were quite clear. The linearity range of amygdalin was 10.25—512.50 μg (r=0.999 9), and the average recovery was 99.78% with RSD of 1.16% (n=6) by HPLC. Conclusion The established method is specific, reproducible, and suitable for the quality control of Anshen Pill.