目的 建立復方川芎滴丸的質(zhì)量標準。方法 采用薄層色譜法對復方中當歸、川芎進行了定性鑒別，采用高效液相色譜法對當歸、川芎中阿魏酸進行了定量測定。結果 薄層色譜分離度好；阿魏酸在0.001～0.100 mg/mL 與峰面積線性關系良好，平均回收率為102.06%，RSD 值為2.25%（n=6）。結論 所建立的方法準確可靠，靈敏度高，專屬性強，可有效控制復方川芎滴丸的質(zhì)量。

Objective To establish the quality standard for Compound Chuanxiong Rhizoma Pills. Methods TLC method was performed to identify Angelica sinensis, Rhizoma Chuanxiong in Compound Rhizoma Chuanxiong Pills and HPLC was used to determine the content of ferulic acid in Angelica sinensis and Chuanxiong Rhizoma. Results TLC had good resolution and specificity. The ferulic acid showed a good liner relationship within the range of 0.001—0.1 mg/mL. The average recovery rate was 102.06% with RSD of 2.25%. Conclusion The method is accurate, specific, and could be used for the quality control of Compound Chuanxiong Rhizoma Pills.

軍隊醫(yī)療機構制劑標準提高科研專項重點課題（13ZJZ02）